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. Author manuscript; available in PMC: 2014 Aug 15.
Published in final edited form as: Tetrahedron Lett. 2013 Jun 18;54(33):4463–4466. doi: 10.1016/j.tetlet.2013.06.041

Table 2.

Yields of reactions in the figure 3

entry glycerol (%)a glycolic acid (%)b formic acid (%)c
B trace 11 39
C trace 20 50
D 19 28 57
E 0 0 61
a

Remaining glycerol/added glycerol × 100.

b

Moles of glycolic acid/moles of added glycerol × 100.

c

(Moles of formic acid/moles of glycerol × 100)/3, assuming one mole of glycerol produced 3 mole of formic acid. Moles of each product were calculated by using methanol as an internal NMR reference.