TABLE 2.
Data collection and refinement statistics
| Data collection | |
|---|---|
| Space group | P41 |
| Cell dimensions | a = b 49.99 and c = 145.86 Å |
| Wavelength (Å) | 0.97315 |
| Resolution (Å) | 1.7 |
| Redundancy | 12.2 (11.9)a |
| I/σ(I) | 40.4 (6.7)a |
| Completeness (%) | 97.2 (94.5)a |
| Rmerge (%) | 6.6 (41.7) |
| Refinement | |
| Resolution (Å) | 25.38-1.70 |
| No. of reflections | 38,239 |
| Rwork/Rfree (%) | 16.5/17.5 |
| No. of atoms | |
| Protein | 2,232 |
| Ligands | 10 |
| Water | 424 |
| B factors | |
| Protein | 18.2 |
| Ligands | 14.6 |
| Water | 32.6 |
| r.m.s.d. | |
| Bond lengths (Å) | 0.006 |
| Bond angles | 1.09° |
| Ramachandran favored (%) | 99 |
| Ramachandran outliers (%) | 0 |
a Numbers in parentheses refer to the highest resolution shell.