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. Author manuscript; available in PMC: 2014 Jul 17.
Published in final edited form as: J Am Chem Soc. 2013 Jul 2;135(28):10198–10201. doi: 10.1021/ja402645y

Figure 1.

Figure 1

Reaction of 0.96 mM 1 with NaBPh4 and Sc(OTf)3 in aerobic CH3CN at 0 °C. (A) UV-visible spectral changes observed with 1 equiv. NaBPh4 and 1 equiv. Sc(OTf)3. Inset: TMC ligand. (B) Plot of the yield of 4 vs. equiv. BPh4 in the presence of 1 equiv. Sc3+. Inset: plot of the yield of 4 vs. equiv. of Sc3+ with 1 equiv. BPh4.