Table 1.
Summary of Data Collection and Refinement Statistics
| HIN-A (Se-SAD) | HIN-B (Native) | |
|---|---|---|
| Data Collection | ||
| Space group | P21 | P212121 |
| Unit cell parameters | ||
| a, b, c (Å) | 43.3, 88.9, 112.8 | 43.0, 92.9, 100.3 |
| α, β, γ (°) | 90.0, 99.4, 90.0 | 90.0, 90.0, 90.0 |
| Wavelength λ(Å) | 0.97918 | 1.0 |
| Rmerge (%) | 7.2 (38.9) | 6.6 (37.9) |
| I/σ (I) | 31.4 (2.7) | 26.4 (4.8) |
| Completeness (%) | 96.4 (85.7) | 99.9 (100) |
| Redundancy | 4.1 (3.6) | 7.2 (7.3) |
| Refinement | ||
| Resolution (Å) | 41.3–2.0 (2.07–2.00) | 42.1–2.35 (2.43–2.35) |
| Number of unique reflections | 55105 | 17421 |
| Rwork/Rfree (%) | 20.8/26.0 | 22.9/29.2 |
| Number of atoms | ||
| Protein | 6160 | 2938 |
| Water | 159 | 17 |
| Mean B factor (Å2) | 47.7 | 55.6 |
| Rms deviation from ideal geometry | ||
| Bond length (Å) | 0.011 | 0.016 |
| Bond angle (°) | 1.332 | 1.466 |
| PDB accession code | 2OQ0 | 3B6Y |
Values in parentheses are for the highest resolution shell.