Table 1.
M2-1 | M2-2 | |||
---|---|---|---|---|
| ||||
δH multi (J) | δ C | δH multi (J) | δ C | |
1 | 2.77 m | 30.3 | 2.77 m | 30.3 |
2 | 2.74 m | 45.7 | 2.74 m | 45.9 |
3 | 211.7 | 211.8 | ||
4 | 2.71 m | 49.6 | 2.71 m | 49.6 |
2.63 m | 2.63 m | |||
5 | 3.12 m | 42.3 | 3.09 m | 41.3 |
6 | 1.53 m | 36.3 | 1.53 m | 36.8 |
7 | 1.39 m | 27.5 | 1.39 m | 27.4 |
8 | 1.28 m | 32.6 | 1.28 m | 32.6 |
9 | 1.33 m | 23.6 | 1.33 m | 23.6 |
10 | 0.891 (7.1) | 14.4 | 0.89 t (7.0) | 144.4 |
1′ | 133.9 | 133.8 | ||
2′ | 6.77 s | 113.2 | 6.76 s | 113.2 |
3′ | 148.9 | 148.9 | ||
4′ | 145.8 | 145.8 | ||
5′ | 6.67 d (8.0) | 116.2 | 6.68 d (8.0) | 116.2 |
6′ | 6.61 d (8.0) | 121.8 | 6.62 d (8.0) | 121.7 |
1″ | a: 3.18 dd (14.5, 3.7) | 32.8 | a: 3.17 dd (14.5, 3.7) | 32.8 |
b: 2.84 dd (14.5, 9.3) | b: 2.85 dd (14.5, 9.3) | |||
2″ | 3.63 m | 56.3 | 3.62 m | 56.3 |
3″ | 172.6 | 172.6 | ||
OMe | 3.82 s | 56.4 | 3.82 s | 56.4 |