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. 2012 Jun 1;43(2):800–809. doi: 10.1590/S1517-83822012000200046

Table 1.

Average degree of polymerization (DP) and fraction of acetylation (FA) of chitosans (Group I) without treatment (A) and thermally treated for 3 and 10 h (B and C) and chitosans (Group II) obtained by partial alkaline deacetylation of chitin (D and E) and chitosans (X1 to X6) generated by partial homogeneous de-N-acetylation of chitin (Group III) and chitosans (Y1 to Y4) obtained by partial re-N-acetylation of polyglucosamine (Group IV).

Group I Group II
Code A B C D E
DP a 1,383 366 45 1,171 1,089
FA 0.22 0.23c 0.22 0.08 0.16
Group III
Code X1 X2 X3 X4 X5 X6
DP b 190 320 68 121 210 224
FA 0.01 0.15 0.35 0.49 0.60 0.69
Group IV
Code Y1 Y2 Y3 Y4
DP a 2,580 2,608 2,528 2,518
FA 0.10 0.29 0.40 0.50
a

DPw (mass average molar mass)

b

DPn (number average molar mass).

c

FA determined by potentiometric titration. FA of other samples were determined by high-field 1H NMR (proton nuclear magnetic resonance spectroscopy)