Table 1.
1H-NMR (200 MHz) data of Cyc A (CDCL 3, 25 ºC).
| Atom | δH | Multi. |
|---|---|---|
| N-CH3 | 3.472 | s |
| 1α | 3.704 | d |
| 1β | 3.687 | m |
| 1γ | 3.662 | d |
| 1γ- CH3 | 0.841 | d |
| 1δ | 1.168 | m |
| 1γ-OH | 3.647 | d |
| 2-NH | 7.264 | d |
| 2α | 3.662 | m |
| 2β | 1.163 | t |
| N-CH3 | 3.378 | s |
| 3α | 3.604 | s |
| N-CH3 | 3.222 | d |
| 4α | 3.444 | t |
| 4β | 1.134 | m |
| 2.982 | m | |
| 4γ | 1.168 | m |
| 4δ1 | 0.841 | d |
| 4δ2 | 1.098 | d |
| 5-NH | 7.264 | d |
| 5α | 3.70 | d |
| 5β | 2.982 | m |
| 5γ1 | 1.098 | d |
| 5γ2 | 1.134 | d |
| N-CH3 | 3.296 | d |
| 6α | 3.704 | t |
| 6β | 1.134 | m |
| 6γ | 1.06 | m |
| 6δ1 | 0.841 | d |
| 6δ2 | 0.841 | d |
| 7-NH | 7.264 | d |
| 7α | 3.687 | m |
| 7β | 1.168 | d |
| 8-NH | 7.268 | d |
| 8α | 3.70 | m |
| 8β | 1.168 | d |
| N-CH3 | 3.164 | d |
| 9α | 3.704 | t |
| 9β | 1.134 | t |
| 9γ | 1.168 | m |
| 9δ1 | 0.841 | d |
| 9δ2 | 0.841 | d |
| N-CH3 | 2.982 | d |
| 10α | 3.70 | t |
| 10β | 1.123 | t |
| 10γ | 1.168 | m |
| 10δ1 | 0.841 | d |
| 10α2 | 0.841 | d |
| N-CH3 | 2.982 | d |
| 11α | 3.704 | d |
| 11β | 1.168 | m |
| 11γ1 | 0.841 | d |
| 11γ2 | 0.841 | d |