| Bruker Kappa APEXII CCD diffractometer | 4910 independent reflections |
| Radiation source: fine-focus sealed tube | 2901 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.031 |
| ω and φ scan | θmax = 27.0°, θmin = 1.8° |
| Absorption correction: multi-scan (SADABS; Bruker, 2004) | h = −12→11 |
| Tmin = 0.977, Tmax = 0.981 | k = −28→28 |
| 16107 measured reflections | l = −13→8 |