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. 2013 Jun 8;69(Pt 7):o1053–o1054. doi: 10.1107/S1600536813014530
C1—C6 1.383 (3) C10—H10D 0.9700
C1—C2 1.386 (3) C11—C12 1.540 (4)
C1—H1 0.9300 C11—H11A 0.9700
C2—C3 1.375 (3) C11—H11B 0.9700
C2—H2 0.9300 C11'—C12 1.516 (8)
C3—C4 1.373 (3) C11'—H11C 0.9700
C3—Cl1 1.742 (2) C11'—H11D 0.9700
C4—C5 1.386 (3) C12—C13 1.487 (3)
C4—H4 0.9300 C12—H12A 0.9700
C5—C6 1.390 (3) C12—H12B 0.9700
C5—H5 0.9300 C12—H12C 0.9700
C6—C7 1.531 (3) C12—H12D 0.9700
C7—C8 1.507 (3) C13—O1 1.387 (2)
C7—C15 1.507 (3) C14—N2 1.319 (3)
C7—H7 0.9800 C14—O1 1.354 (2)
C8—C13 1.321 (3) C14—C15 1.379 (3)
C8—C9 1.480 (3) C15—N1 1.381 (3)
C9—O2 1.212 (3) C16—N2 1.444 (3)
C9—C10 1.494 (3) C16—H16A 0.9600
C10—C11 1.475 (4) C16—H16B 0.9600
C10—C11' 1.489 (8) C16—H16C 0.9600
C10—H10A 0.9700 N1—O4 1.241 (2)
C10—H10B 0.9700 N1—O3 1.264 (2)
C10—H10C 0.9700 N2—H2A 0.901 (10)
C6—C1—C2 121.4 (2) C12—C11—H11A 109.1
C6—C1—H1 119.3 C10—C11—H11B 109.1
C2—C1—H1 119.3 C12—C11—H11B 109.1
C3—C2—C1 118.5 (2) H11A—C11—H11B 107.8
C3—C2—H2 120.7 C10—C11'—C12 113.0 (6)
C1—C2—H2 120.7 C10—C11'—H11C 109.0
C4—C3—C2 122.0 (2) C12—C11'—H11C 109.0
C4—C3—Cl1 119.25 (19) C10—C11'—H11D 109.0
C2—C3—Cl1 118.77 (18) C12—C11'—H11D 109.0
C3—C4—C5 118.7 (2) H11C—C11'—H11D 107.8
C3—C4—H4 120.7 C13—C12—C11' 114.3 (4)
C5—C4—H4 120.7 C13—C12—C11 109.3 (2)
C4—C5—C6 121.05 (19) C13—C12—H12A 109.8
C4—C5—H5 119.5 C11'—C12—H12A 132.3
C6—C5—H5 119.5 C11—C12—H12A 109.8
C1—C6—C5 118.42 (19) C13—C12—H12B 109.8
C1—C6—C7 120.98 (18) C11'—C12—H12B 72.9
C5—C6—C7 120.58 (17) C11—C12—H12B 109.8
C8—C7—C15 108.83 (16) H12A—C12—H12B 108.3
C8—C7—C6 110.16 (16) C13—C12—H12C 108.6
C15—C7—C6 112.73 (16) C11'—C12—H12C 109.1
C8—C7—H7 108.3 C11—C12—H12C 138.6
C15—C7—H7 108.3 H12A—C12—H12C 71.7
C6—C7—H7 108.3 C13—C12—H12D 108.6
C13—C8—C9 118.77 (19) C11'—C12—H12D 108.6
C13—C8—C7 123.07 (18) C11—C12—H12D 75.4
C9—C8—C7 118.15 (18) H12B—C12—H12D 136.4
O2—C9—C8 120.0 (2) H12C—C12—H12D 107.5
O2—C9—C10 122.1 (2) C8—C13—O1 122.63 (18)
C8—C9—C10 117.8 (2) C8—C13—C12 126.9 (2)
C11—C10—C9 114.4 (2) O1—C13—C12 110.45 (18)
C11'—C10—C9 119.7 (4) N2—C14—O1 111.88 (18)
C11—C10—H10A 108.7 N2—C14—C15 127.66 (19)
C11'—C10—H10A 129.7 O1—C14—C15 120.45 (18)
C9—C10—H10A 108.7 C14—C15—N1 120.21 (18)
C11—C10—H10B 108.7 C14—C15—C7 123.32 (18)
C11'—C10—H10B 70.3 N1—C15—C7 116.47 (17)
C9—C10—H10B 108.7 N2—C16—H16A 109.5
H10A—C10—H10B 107.6 N2—C16—H16B 109.5
C11—C10—H10C 72.8 H16A—C16—H16B 109.5
C11'—C10—H10C 107.4 N2—C16—H16C 109.5
C9—C10—H10C 107.4 H16A—C16—H16C 109.5
H10B—C10—H10C 138.8 H16B—C16—H16C 109.5
C11—C10—H10D 136.3 O4—N1—O3 120.52 (18)
C11'—C10—H10D 107.4 O4—N1—C15 118.43 (18)
C9—C10—H10D 107.4 O3—N1—C15 121.05 (18)
H10A—C10—H10D 67.7 C14—N2—C16 125.1 (2)
H10C—C10—H10D 106.9 C14—N2—H2A 110.2 (17)
C10—C11—C12 112.5 (2) C16—N2—H2A 124.7 (17)
C10—C11—H11A 109.1 C14—O1—C13 119.69 (16)
C6—C1—C2—C3 0.9 (3) C10—C11'—C12—C13 −33.1 (11)
C1—C2—C3—C4 0.1 (3) C10—C11'—C12—C11 57.6 (6)
C1—C2—C3—Cl1 −178.49 (17) C10—C11—C12—C13 46.9 (3)
C2—C3—C4—C5 −0.9 (3) C10—C11—C12—C11' −58.2 (6)
Cl1—C3—C4—C5 177.67 (16) C9—C8—C13—O1 175.11 (18)
C3—C4—C5—C6 0.7 (3) C7—C8—C13—O1 −4.1 (3)
C2—C1—C6—C5 −1.1 (3) C9—C8—C13—C12 −4.8 (3)
C2—C1—C6—C7 177.64 (19) C7—C8—C13—C12 176.0 (2)
C4—C5—C6—C1 0.3 (3) C11'—C12—C13—C8 20.5 (7)
C4—C5—C6—C7 −178.48 (18) C11—C12—C13—C8 −20.3 (3)
C1—C6—C7—C8 −119.8 (2) C11'—C12—C13—O1 −159.3 (6)
C5—C6—C7—C8 58.9 (2) C11—C12—C13—O1 159.8 (2)
C1—C6—C7—C15 118.4 (2) N2—C14—C15—N1 0.5 (3)
C5—C6—C7—C15 −62.8 (2) O1—C14—C15—N1 −179.05 (18)
C15—C7—C8—C13 13.3 (3) N2—C14—C15—C7 −179.6 (2)
C6—C7—C8—C13 −110.8 (2) O1—C14—C15—C7 0.9 (3)
C15—C7—C8—C9 −166.00 (17) C8—C7—C15—C14 −11.7 (3)
C6—C7—C8—C9 69.9 (2) C6—C7—C15—C14 110.8 (2)
C13—C8—C9—O2 −174.9 (2) C8—C7—C15—N1 168.27 (17)
C7—C8—C9—O2 4.4 (3) C6—C7—C15—N1 −69.2 (2)
C13—C8—C9—C10 3.3 (3) C14—C15—N1—O4 176.39 (19)
C7—C8—C9—C10 −177.4 (2) C7—C15—N1—O4 −3.6 (3)
O2—C9—C10—C11 −156.9 (3) C14—C15—N1—O3 −3.9 (3)
C8—C9—C10—C11 24.9 (3) C7—C15—N1—O3 176.11 (18)
O2—C9—C10—C11' 159.0 (6) O1—C14—N2—C16 4.2 (3)
C8—C9—C10—C11' −19.1 (7) C15—C14—N2—C16 −175.4 (2)
C11'—C10—C11—C12 57.4 (6) N2—C14—O1—C13 −169.49 (18)
C9—C10—C11—C12 −50.4 (4) C15—C14—O1—C13 10.1 (3)
C11—C10—C11'—C12 −59.2 (7) C8—C13—O1—C14 −8.7 (3)
C9—C10—C11'—C12 33.9 (11) C12—C13—O1—C14 171.21 (19)