Bruker SMART APEXII CCD diffractometer | 2786 independent reflections |
Radiation source: fine-focus sealed tube | 2208 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.029 |
ω and φ scans | θmax = 25.0°, θmin = 2.2° |
Absorption correction: multi-scan (SADABS; Bruker, 2008) | h = −9→8 |
Tmin = 0.912, Tmax = 0.924 | k = −12→12 |
11848 measured reflections | l = −15→21 |