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. Author manuscript; available in PMC: 2013 Sep 19.
Published in final edited form as: Chem Commun (Camb). 2012 Jan 30;48(19):2546–2548. doi: 10.1039/c2cc16277f

Scheme II.

Scheme II

Synthetic route to [MII2H4bnppap(OH)2]+ (M = CoII, MnII). Conditions: (a) 3 equiv NaH, (b) 2 equiv Co(NO3)2·6H2O or Mn(OTf)2·2MeCN (c) 2 equiv of H2O (d) 1 equiv NaBPh4.