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. 2013 Aug 5;135(36):13440–13445. doi: 10.1021/ja405103r

Figure 2.

Figure 2

Typical 13C NMR of the homogeneous DHF/glyoxylate (without cyanide) reaction. Reaction of 0.25 M glyoxylate with 0.25 M DHF in aqueous 1.0 M NaOH and 1M LiOH (room temperature, 1 h). For NMR details see caption of Figure 1.