Skip to main content
. Author manuscript; available in PMC: 2014 Sep 17.
Published in final edited form as: Acc Chem Res. 2013 Jul 26;46(9):2127–2135. doi: 10.1021/ar4000482

Figure 5.

Figure 5

(a) The aliphatic region of a 2D 13C/13C correlation SSNMR spectrum and (b) sequential assignments by 3D (purple) NCOCA and (red) CANCO spectra of GB1 micro-crystal sample incubated with 30 mM Cu2+-EDTA. The data were collected at the 1H frequency of 750 MHz using the PACC approach with a recycle delay of 300 ms using a Bruker 1.3 mm CPMAS triple-resonance probe. The experimental times were (a) 15 min and (b) 1 hour for each 3D data.