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Results for the copolymerization of DEAAm and DMAEMA using different monomer ratios.
| DEAAm/DMAEMA | conc. [wt %] |
AIBN [mol %] |
temp. [°C] |
time [h] |
conversion [%] |
Mn,GPC [g mol−1] |
PDI |
| 1:1 | 25 | 0.5 | 60 | 18 | >99 | 37200 | 3.20 |
| 5:1 | 25 | 0.5 | 60 | 18 | >99 | 71500 | 2.72 |
| 1:1 | 50 | 0.5 | 60 | 18 | >99 | 57100 | 4.47 |
| 5:1 | 50 | 0.5 | 60 | 18 | >99 | 121400 | 3.27 |
| 1:1 | bulk | 0.25 | varyinga | varyinga | >99 | 187400 | 4.30 |
a16 h at 60 °C, 8 h at 70 °C, 16 h at 80 °C, and 3 h at 100 °C.
