Table 2. Amounts of Ammoxidation Products (mg Product/100 mg of Educt) in the EtOAc Extracts (Optimized Protocol), Aqueous Phases, and Water-Insoluble Fraction.

EtOAc extract	water soluble	water insoluble	ammoxidation conditionsa	EtOAc extract	water soluble	water insoluble
Glucose				Cellulose
0	104	0	RT, ambient pressure	0.1	2	93.7
1.8	67.5	0	70 °C	0.4	2.1	89.6
14.0	77.2	0.6	100 °C	0.9	2.1	91.9
13.0	65.6	6.8	140 °C	1.2	9.8	89.9
Xylose				Xylan
0	71.0	0	RT, ambient pressure	0.1	39.0	59.1
3.4	91.1	0	70 °C	0	77.4	11.7
n.d.	82.5	0	100 °C	0.2	26.3	68.5
17.7	71.9	2.3	140 °C	3.9	43.5	41.4

^aAqueous ammonia (5 w%), 0.2 MPa oxygen partial pressure, 3 h of reaction time.