Bruker APEX CCD diffractometer | 4078 independent reflections |
Radiation source: fine-focus sealed tube | 3384 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.032 |
φ and ω scans | θmax = 26.0°, θmin = 1.9° |
Absorption correction: multi-scan (SADABS; Bruker, 2001) | h = −47→47 |
Tmin = 0.307, Tmax = 0.457 | k = −6→6 |
14961 measured reflections | l = −26→26 |