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. 2013 Sep 21;69(Pt 10):m556–m557. doi: 10.1107/S160053681302518X
Bruker APEX CCD diffractometer 4078 independent reflections
Radiation source: fine-focus sealed tube 3384 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.032
φ and ω scans θmax = 26.0°, θmin = 1.9°
Absorption correction: multi-scan (SADABS; Bruker, 2001) h = −47→47
Tmin = 0.307, Tmax = 0.457 k = −6→6
14961 measured reflections l = −26→26