| Stoe IPDS2 diffractometer | 5771 independent reflections |
| Radiation source: fine-focus sealed tube | 4259 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.070 |
| Detector resolution: 6.67 pixels mm-1 | θmax = 29.2°, θmin = 2.2° |
| ω scans | h = −24→23 |
| Absorption correction: numerical (X-AREA; Stoe & Cie, 2002) | k = −15→16 |
| Tmin = 0.727, Tmax = 0.883 | l = −17→17 |
| 10087 measured reflections |
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