| Bruker SMART APEXII CCD diffractometer | 5042 independent reflections |
| Radiation source: fine-focus sealed tube | 3610 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.023 |
| ω and φ scans | θmax = 26.5°, θmin = 1.9° |
| Absorption correction: multi-scan (SADABS; Bruker, 2008) | h = −13→13 |
| Tmin = 0.986, Tmax = 0.986 | k = −14→14 |
| 18615 measured reflections | l = −15→15 |
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