| Bruker SMART APEX CCD diffractometer | 3374 independent reflections |
| Radiation source: fine-focus sealed tube | 2889 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.043 |
| Detector resolution: 8.3660 pixels mm-1 | θmax = 29.1°, θmin = 2.4° |
| φ and ω scans | h = −10→10 |
| Absorption correction: multi-scan (SADABS; Bruker, 2013) | k = −23→23 |
| Tmin = 0.84, Tmax = 1.00 | l = −13→13 |
| 22947 measured reflections |
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