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Transmission electron microscopy (TEM) image of palladium particles after 0.25 h of dehydrogenating 3-methylcyclohexanone. Reaction conditions: [ketone] = 2 M (1 mmol), [Pd(TFA)2] = 0.06 M (0.03 mmol), [2-Me2Npy] = 0.12 M (0.06 mmol), [TsOH] = 0.24 M (0.12 mmol), DMSO for VTotal of 0.5 mL, 1 atm O2, 80 °C.
