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. Author manuscript; available in PMC: 2014 Jun 5.
Published in final edited form as: J Am Chem Soc. 2013 May 24;135(22):8213–8221. doi: 10.1021/ja403165u

Figure 9.

Figure 9

Palladium particle sizes at different reaction times for the dehydrogenation of (A) 3-methylcyclohexanone and (B) 3-methylcyclohexenone at 5 min and 2 h. Reaction conditions: [ketone] = 2 M (1 mmol), [Pd(TFA)2] = 0.06 M (0.03 mmol), [2-Me2Npy] = 0.12 M (0.06 mmol), [TsOH] = 0.24 M (0.12 mmol), DMSO for VTotal of 0.5 mL, 1 atm O2, 80 °C.