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. Author manuscript; available in PMC: 2014 Sep 21.
Published in final edited form as: Analyst. 2013 Jul 24;138(18):5384–5395. doi: 10.1039/c3an01174g

Table 1.

Average lattice parameters and standard deviations (in Å) of mesophases at 25 ± 1 °C in samples prepared and analysed on-chip and in samples prepared using coupled syringes and analysed in glass capillaries. Chips A–D are the same as those in Figure 5.

Sample composition
MO/5% βOG
55:45 v/v
MO/6.7% βOG
55:45 v/v
MO/8.3% βOG
55:45 v/v
MO/10% βOG
55:45 v/v

Detergent solutions and mesophases formulated on-chipa
Pn3m Ia3d b Pn3m Ia3d b Pn3m Ia3d b Pn3m Ia3d b
Chip A 182 ± 2 185 ± 3 49.2 136 ± 1 215 ± 12 49.9 144 ± 3 49.8
Chip B 187 ± 3 49.1 183 ± 6 48.9 136 ± 1 190 49.7 146 ± 2 49.7
Chip C 181 ± 2 48.9 198 ± 1 49.5 143 ± 3 191 49.9 144 ± 2 49.7
Chip D 179 ± 1 193 ± 2 49.8 141 ± 2 215 ± 3 50.1 145 ± 2 50.0

Detergent solutions formulated off-chip, mesophases formulated on-chipc
Chip E 181 ± 2 48.6
Chip F 182 ± 3 48.9
Chip G 148 ± 3 49.8
Chip H 148 ± 8 49.7

Samples prepared in coupled syringes and analyzed in glass capillaries
CS-1 177 ± 2 48.4
CS-2 173 ± 1 49.9
a

Lattice parameters were averaged for each of the four samples on-chip

b

Standard deviations of lattice parameters for phases were <0.5 Å in all cases.

c

Four identical samples were prepared on a single chip. The reported value is the average for the four samples.