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Hyperfine shifted NMR resonance of 1 mM unlabeled-KpFeoC detected by superWEFT pulse sequence. (A) 1H spectra of native state (mostly oxidized, top trace) and the dithionite-reduced state (bottom trace). (B) 13C spectra of 1.3 mM [U-13C, 15N]-KpFeoC at native state at 283 K (top trace) and 278 K (bottom trace). The recycle delay times for the superWEFT sequence were ∼0.1 and ∼0.2 s for proton and carbon spectra, respectively.
