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. 2004 Feb 26;23(5):1030–1039. doi: 10.1038/sj.emboj.7600139

Table 1.

Data collection and refinement statistics

Data collection statistics  
Cell parameters 157.7 Å; 157.7 Å; 243.2 Å; 90°; 90°; 120°
Space group P65
Wavelength 0.9394 Å
Resolution max. 2.9 Å
Completeness (last shell) 96.3% (99.3%)
Rmerge (last shell) 9.6% (58.0%)
Redundancy 6.9
II 10.5 (3.1)
   
Refinement
Resolution range 40–2.9 Å
No. of reflections 72860 (6732 in test set)
R-factor 24.8%
Rfree 29.5%
No. of residues 2871
No. of ADP 6
Solvent 63
Ramachandran plot  
Most favoured regions 81.7%
Add. allowed regions 16.8%
Disallowed regions
0.2%
Rmerge=∑hkliI(hkl)i−〈I(hkl)〉∣/∑hkliI(hkl)i.
R-factor=∑hklFo(hkl)−Fc(hkl)∣/∑hklFo(hkl)∣, where Fo and Fc are observed and calculated structure factors, respectively.
HHS Vulnerability Disclosure