Table 2.
Compound | Condition | Concentration (ng/mL) | RSD | RE |
---|---|---|---|---|
Added | (%) | (%) | ||
Morphine | Three freeze–thaw cycles | 50 | 2.5 | −10.1 |
200 | 1.4 | −8.9 | ||
1600 | 4.3 | −12.5 | ||
Autosampler ambient 12 h | 50 | 2.1 | −10.5 | |
200 | 1.3 | −6.2 | ||
1600 | 3.5 | −9.2 | ||
| ||||
Codeine | Three freeze–thaw cycles | 50 | 3.2 | −8.9 |
200 | 3.3 | −11.2 | ||
1600 | 3.0 | −14.1 | ||
Autosampler ambient 12 h | 50 | 3.3 | −11.1 | |
200 | 3.2 | −12.9 | ||
1600 | 3.3 | −14.4 |