Table 2.
XRPD peak parameters of GLP and formulations.
| Batch | Precipitated NCs |
Complexed NCs |
||||
|---|---|---|---|---|---|---|
| 2θ position | Peak intensity (d) | FWHM (deg) | 2θ position | Peak intensity (d) | FWHM (deg) | |
| Pure GLP | 17.82 | 4.97 | – | – | – | – |
| 20.77 | 4.27 | – | – | – | – | |
| 22.68 | 3.91 | – | – | – | – | |
| 24.91 | 3.57 | – | – | – | – | |
| 26.02 | 3.42 | – | – | – | – | |
| 53.82 | 1.70 | – | – | – | – | |
| F1 | 20.77 | 4.27 | – | 18.92 | 4.66 | 0.42 |
| 22.64 | 3.92 | – | – | – | – | |
| 24.91 | 3.57 | – | 23.55 | 3.77 | 3.31 | |
| 26.00 | 3.42 | – | 28.43 | 3.13 | – | |
| 53.73 | 1.70 | – | – | – | – | |
| F2 | 18.02 | 4.91 | – | 18.90 | 4.66 | 0.36 |
| 20.92 | 4.23 | – | – | – | – | |
| 25.11 | 3.54 | – | 23.66 | 3.75 | 0.43 | |
| 26.23 | 3.39 | – | – | – | – | |
| F3 | 17.92 | 4.94 | – | – | – | – |
| 18.92 | 4.63 | – | 19.01 | 4.66 | 0.34 | |
| 20.80 | 4.25 | – | 20.70 | 4.41 | 0.32 | |
| 22.78 | 3.90 | – | 23.63 | 3.76 | 0.34 | |
| 25.0 | 3.5 | – | – | – | – | |
| 26.10 | 3.41 | – | – | – | – | |
| F4 | 18.04 | 4.91 | 0.28 | 19.06 | 4.65 | 0.43 |
| 20.97 | 4.23 | 0.33 | – | – | – | |
| 22.89 | 3.88 | – | 23.67 | 3.75 | 0.38 | |
| 26.24 | 3.39 | 0.30 | – | – | – | |
| 22.51 | 3.93 | – | – | – | – | |
| F5 | 24.84 | 3.58 | – | 21.60 | 11.24 | 0.41 |
| 25.94 | 3.43 | – | 24.41 | 2.67 | 0.38 | |
FWHM – full width half maximum.