Skip to main content
. 2013 Nov 4;8(11):e77995. doi: 10.1371/journal.pone.0077995

Table 1. Data collection and refinement statistics of OPHC2 structures.

Data collection
PDB ID 4LE6
Beamline PROXIMA-1
Wavelength (Å) 0.980
Detector PILATUS 6M
Oscillation (°) 0.15
Number of frames 1200
Resolution (Å) (last bin) 2.1 (2.2–2.1)
Space group C2
Unit-cell parameters (Å) a = 109.9, b = 63.8,c = 221.3, β = 101.8
No. of observed reflections (last bin) 252270 (24317)
No. of unique reflections (last bin) 82530 (9469)
Completeness (%)(last bin) 93.7 (82.6)
Rmeas (%) (last bin) 6.5 (50.1)
I/σ(I) (last bin) 13.67 (3.07)
Redundancy (last bin) 3.06 (2.57)
Mosaicity (°) 0.508
Refinement statistics
Rfree/Rwork 20.99/17.32
No. of total model atoms 19946
Ramachandran favored 93.5
Ramachandran outliers 0.8
Generously allowed rotamers 5.7
Rmsd from ideal
Bond lengths (Å) 0.008
Bond angles (°) 1.111