Table 2.
Results of the evaluation of the precision of the system.
| Content [%] | |||||
|---|---|---|---|---|---|
| No. of the sample | I5 R t = 24.9′ |
I6 R t = 29.8′ |
U2 R t = 23.1′ |
U5 R t = 26.8′ |
U6 R t = 31.3′ |
| 1 | 0.03 | 0.11 | 0.09 | 0.75 | 0.16 |
| 2 | 0.03 | 0.09 | 0.09 | 0.72 | 0.13 |
| 3 | 0.03 | 0.13 | 0.07 | 1.01 | 0.14 |
| 4 | 0.03 | 0.13 | 0.07 | 1.08 | 0.14 |
| 5 | 0.03 | 0.12 | 0.06 | 0.58 | 0.13 |
| 6 | 0.02 | 0.10 | 0.07 | 0.54 | 0.11 |
| 7 | 0.03 | 0.11 | 0.07 | 0.63 | 0.11 |
| 8 | 0.04 | 0.13 | 0.08 | 0.97 | 0.14 |
|
| |||||
| X | 0.03 | 0.12 | 0.08 | 3.28 | 0.15 |
| SD | 0.03 | 0.12 | 0.08 | 1.26 | 0.14 |
| RSD | 0.005 | 0.02 | 0.01 | 1.05 | 0.02 |
I5 and I6: identified impurities; U2, U5, U6: unidentified impurities; R t: retention time; X: average; SD: standard deviation; and RSD: relative standard deviation.