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. Author manuscript; available in PMC: 2013 Nov 7.
Published in final edited form as: Aust J Chem. 2010 Jun 11;63(6):10.1071/CH10068. doi: 10.1071/CH10068

Table 1.

13C NMR spectroscopic data for saliniquinones A–F (1–6, in CDCl3)A

Position Compound δC
1 2 3 4 5 6
2 168.9 169.9 169.6 165.6 170.1 171.6
3 109.8 109.0 110.7 108.5 113.0 109.7
4 179.7 179.8 179.7 180.3 178.7 179.4
4a 126.6 126.6 126.3 126.4 126.5 126.3
5 150.2 150.0 150.2 149.6 150.3 150.4
6 124.0 124.0 124.0 123.5 126.0 126.0
6a 136.9 NRB NRB NRB 135.9 136.0
7 181.4 181.4 181.1 181.5 181.7 181.9
7a 132.3 132.1 132.0 132.1 132.3 132.1
8 119.9 119.8 119.8 119.5 119.6 119.5
9 137.3 136.9 137.1 136.6 136.8 136.6
10 125.8 125.7 125.6 125.6 125.5 125.4
11 162.8 162.8 162.8 162.7 162.6 162.6
11a 116.8 116.7 116.4 116.6 116.6 116.7
12 187.0 187.1 187.1 187.2 187.6 187.4
12a 121.6 121.5 121.0 121.4 119.5 119.6
12b 156.6 156.6 155.9 156.4 156.5 156.1
13 65.2 65.2 64.9 65.1 24.4 24.1
14 59.6 57.9 75.7 125.7 44.7 72.9
15 14.0 13.7 25.0 12.3 15.8 26.3
16 66.1 67.7 68.7 142.9 74.5 45.2
17 130.9 22.0 133.2 22.7 138.5 131.8
18 123.1 10.4 120.3 13.3 116.4 120.8
A

Chemical shifts (δ) in ppm.

B

Resonances were not observed.