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. Author manuscript; available in PMC: 2014 Jun 1.

Published in final edited form as: J Struct Funct Genomics. 2013 May 25;14(2):10.1007/s10969-013-9155-9. doi: 10.1007/s10969-013-9155-9

Table 1. X-ray data and refinement statistics for Gl-MIF.

Crystal parameters	Iodide	Native
Space group	I2₁3	I2₁3
Cell dimensions a=b=c (Å), α=β=γ	95.6, 90	95.55; 90
Data set
X-ray source	X29A, NSLS	23-IDD, APS
Wavelength (Å)	1.54	0.97934
Resolution (Å)	50–2.6 (2.67–2.60)	50–2.30 (2.36–2.30)
Rmerge	0.044 (0.529)	0.032 (0.441)
I/sigma (I)	71.0 (9.3)	33.9 (4.4)
Completeness	100 % (100 %)	100 % (100 %)
# reflections overall	198,979 (15,450)	47,688 (6,594)
# reflections, unique	4,744 (359)	6,594 (494)
Multiplicity	42 (43)	7.2 (7.3)
Phasing statistics
FOM (PHASER, 50–2.6 Å)	0.39
FOM (PARROT, 50-2.6Å)	0.64
Refinement statistics
R_work		0.223
R_free		0.268
RMSD bond lengths (Å)		0.012
RMSD bond angles (Å)		1.63
Ramachandran:
Preferred (%)		91 (97.9 %)
Allowed (%)		2 (2.1 %)
Disallowed		0 (0 %)
Molprobity clash score		7.65 (97th)
Molprobity score		1.75 (97th)