Table 1.
1H-NMR and 13C-NMR data for the pentacyclic triterpenes in Euphorbia microsciadiaa
C |
1
|
2
|
3
|
---|---|---|---|
13 C- NMR | 13 C- NMR | 13 C- NMR | |
1 | 38.6 t | 39.1 t | 38.78 t |
2 | 27.0 t | 27.9 t | 23.4 t |
3 | 78.7 d | 79.7 d | 79.0 d |
4 | 38.7 s | 40.0 s | 39.5 s |
5 | 55.3 d | 55.9 d | 55.2 d |
6a | 18.2 t | 19.1 t | 18.2 t |
7a | 34.2 t | 33.4 t | 33.0 t |
8 | 40.5 s | 40.2 s | 39.0 s |
9 | 50.4 d | 48.32 d | 47.6 d |
10 | 37.0 s | 37.8 s | 36.6 s |
11 | 20.8 t | 24.0 t | 23.7 t |
12 | 25.4 t | 123.3 d | 125.7 d |
13 | 38.2 d | 143.3 s | 137.9 s |
14 | 42.3 s | 42.4 s | 41.9 s |
15 | 30.5 t | 28.4 t | 29.3 t |
16 | 32.1 t | 24.1 t | 23.3 t |
17 | 56.1 s | 46.6 s | 47.9 s |
18 | 49.1 d | 41.9 d | 52.7 d |
19 | 46.9 d | 46.6 t | 30.6 d |
20 | 150.6 s | 30.4 s | 30.3 d |
21 | 37.0 t | 34.5 t | 27.2 t |
22 | 29.6 t | 31.3 t | 37.0 t |
23 | 27.5 q | 28.8 q | 23.4 q |
24 | 15.2 q | 16.2 q | 16.9 q |
25 | 15.8 q | 16.0 q | 16.9 q |
26 | 16.0 q | 17.7 q | 15.4 q |
27 | 14.5 q | 26.6 q | 24.2 q |
28 | 189.1 s | 172.0 s | 175.9 q |
29 | 106.4 t | 33.7 q | 21.0 q |
30 | 19.2 q | 24.2 q | 23.3 q |
Chemical shifts are given in ppm