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. 2013 Nov 15;46(Pt 6):1823–1833. doi: 10.1107/S0021889813027751

Table 2. Parameters derived from the Guinier analyses of the hpHMW-FG SE-HPLC-SAXS data with baseline subtraction and Gaussian decomposition.

Values in parentheses are the uncertainties on the least significant digits derived from the linear regression standard deviations.

G-pk [frames averaged] c (average) (mg ml−1) [〈R g 2z]1/2 (Å) Mw (kg mol−1) q min−1) q max−1) Points used Fit St. Er. (average) [〈R c 2z]1/2 (Å) M/Lw/z (g mol−1 Å−1) q min−1) q max−1) Points used Fit St. Er. (average)
1 [73–85] 0.043 278.2 (131) 5040 (18) 0.0033 0.0043 5 0.0138 141.6 (23) 5105 (56) 0.0045 0.0068 10 0.0078
17.1 (20) 446 (27) 0.0350 0.0499 57 0.1056
2 [81–95] 0.091 200.2 (19) 2205 (18) 0.0040 0.0063 10 0.0065 97.9 (10) 3376 (26) 0.0078 0.0101 10 0.0036
17.9 (15) 462 (23) 0.0388 0.0499 45 0.0516
3 [111–130] 0.101 202.6 (36) 685.6 (83) 0.0033 0.0058 11 0.0126 18.4 (04) 565 (7) 0.0318 0.0499 73 0.0321
4 [159–174] 0.587 133.8 (9) 320.3 (13) 0.0033 0.0088 23 0.0082 15.5 (2) 528 (3) 0.0318 0.0499 73 0.0120
5 [173–183] 0.166 132.1 (13) 342.0 (26) 0.0056 0.0098 18 0.0100 15.5 (4) 576 (6) 0.0318 0.0499 73 0.0229
6 [185–200] 0.537 131.2 (8) 358.0 (12) 0.0053 0.0083 13 0.0031 16.1 (2) 620 (4) 0.0318 0.0499 73 0.0116
  [311 (30)]

From an 〈Mw versus c linear fit of frames 193–199.