Table 2. Parameters derived from the Guinier analyses of the hpHMW-FG SE-HPLC-SAXS data with baseline subtraction and Gaussian decomposition.
Values in parentheses are the uncertainties on the least significant digits derived from the linear regression standard deviations.
| G-pk [frames averaged] | c (average) (mg ml−1) | [〈R g 2〉z]1/2 (Å) | 〈M〉w (kg mol−1) | q min (Å−1) | q max (Å−1) | Points used | Fit St. Er. (average) | [〈R c 2〉z]1/2 (Å) | 〈M/L〉w/z (g mol−1 Å−1) | q min (Å−1) | q max (Å−1) | Points used | Fit St. Er. (average) |
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| 1 [73–85] | 0.043 | 278.2 (131) | 5040 (18) | 0.0033 | 0.0043 | 5 | 0.0138 | 141.6 (23) | 5105 (56) | 0.0045 | 0.0068 | 10 | 0.0078 |
| 17.1 (20) | 446 (27) | 0.0350 | 0.0499 | 57 | 0.1056 | ||||||||
| 2 [81–95] | 0.091 | 200.2 (19) | 2205 (18) | 0.0040 | 0.0063 | 10 | 0.0065 | 97.9 (10) | 3376 (26) | 0.0078 | 0.0101 | 10 | 0.0036 |
| 17.9 (15) | 462 (23) | 0.0388 | 0.0499 | 45 | 0.0516 | ||||||||
| 3 [111–130] | 0.101 | 202.6 (36) | 685.6 (83) | 0.0033 | 0.0058 | 11 | 0.0126 | 18.4 (04) | 565 (7) | 0.0318 | 0.0499 | 73 | 0.0321 |
| 4 [159–174] | 0.587 | 133.8 (9) | 320.3 (13) | 0.0033 | 0.0088 | 23 | 0.0082 | 15.5 (2) | 528 (3) | 0.0318 | 0.0499 | 73 | 0.0120 |
| 5 [173–183] | 0.166 | 132.1 (13) | 342.0 (26) | 0.0056 | 0.0098 | 18 | 0.0100 | 15.5 (4) | 576 (6) | 0.0318 | 0.0499 | 73 | 0.0229 |
| 6 [185–200] | 0.537 | 131.2 (8) | 358.0 (12) | 0.0053 | 0.0083 | 13 | 0.0031 | 16.1 (2) | 620 (4) | 0.0318 | 0.0499 | 73 | 0.0116 |
| [311 (30)]† |
From an 〈M〉w versus c linear fit of frames 193–199.