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Additional details of the data collection and structure refinement of K[endo-Re(CO)3(rac-ASMA)].
| 2B and 4B | |
|---|---|
| empirical formula | C9H7KNO9Re |
| formula weight | 498.46 |
| T (K) | 173 (2) |
| λ (Å) | 0.71073 |
| crystal system | monoclinic |
| space group | P21/c |
| unit cell dimensions | |
| a (Å) | 7.952 (4) |
| b (Å) | 14.774 (7) |
| c (Å) | 10.879 (5) |
| β (deg) | 98.417 (7) |
| V (Å3) | 1264.4 (10) |
| Z | 4 |
| ρcalc (mg/m3) | 2.619 |
| abs coeff (mm−1) | 9.988 |
| R indices [I > 2σ(I)] | R1 = 0.0260 |
| wR2 = 0.0590 |
