Table 1.
Gradient Used for Elution of Pigments by HPLC Reverse Phasea
time (min) | solvent A | solvent B | solvent C | flow (mL/min) | curve |
---|---|---|---|---|---|
0.00 | 75.0 | 25.0 | 0.0 | 1.25 | 1 |
8.00 | 25.0 | 75.0 | 0.0 | 1.25 | 6 |
10.00 | 25.0 | 0.0 | 75.0 | 1.25 | 6 |
11.00 | 19.0 | 0.0 | 81.0 | 1.25 | 6 |
13.00 | 14.0 | 0.0 | 86.0 | 1.25 | 6 |
15.00 | 11.0 | 0.0 | 89.0 | 1.25 | 6 |
16.00 | 0.0 | 0.0 | 100.0 | 1.25 | 6 |
18.00 | 0.0 | 0.0 | 100.0 | 1.25 | 6 |
20.00 | 75.0 | 25.0 | 0.0 | 1.25 | 1 |
(1/1/8) (v/v/v) water/ammonium acetate 1 M/methanol (solvent A), acetonitrile (solvent B), and reagent alcohol (solvent C).