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Thermal characterization of prazosin salts.
| Salt | Tm (K)# | Tg (K)# | Tm/Tg | Ea (kJ/mol) | Tc (K)* | RCT$ |
|---|---|---|---|---|---|---|
| PRB MES-AM | 540.13 | 433.4 | 1.25 | 448.5 | 453.0 | 0.16 |
| PRB TSA-AM | 573.13 | 400.6 | 1.45 | 490.7 | 428.0 | 0.18 |
| PRB HCl-AM | 545.13 | 399.7 | 1.38 | 206.1 | 402.0 | 0.01 |
heating rate: 3 K/min; Tm: melting temperature (onset); Tg: glass transition (midpoint-inflection);
reduced crystallization temperature.
