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. Author manuscript; available in PMC: 2014 Oct 10.
Published in final edited form as: J Med Chem. 2013 Sep 19;56(19):10.1021/jm401184f. doi: 10.1021/jm401184f

Table 6.

HPLC conditions for [18F]7a and [18F]7c

Column Mobile phase Flow rate,
mL/min		 Product
retention
time, min		 Nitro
precursor
retention
time, min
[18F]7a, preparative XBridge C18 column, 10 µm (250 × 10 mm) CH3OH/CH3CN/H2O/Me3N 260:120:620:2 12 32 21
[18F]7a, analytical XBridge C18 column, 5 µm (250 × 4.6 mm) CH3CN/H2O/Et3N 390:610:1 2 7.4 5.5
[18F]7c, preparative XBridge C18 column, 10 µm (150 × 10 mm) CH3CN/H2O/NH3 280:720:1 10 20 27
[18F]7c, analytical XBridge C18 column, 3.5 µm (100 × 4.6 mm) CH3CN/H2O/NH3 380:620:1 2 3.4 5.2