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. 2013 Nov 1;9:2336–2343. doi: 10.3762/bjoc.9.268

Figure 5.

Figure 5

ORTEP drawing of 12. Thermal ellipsoids are set at 35% probability level. Hydrogen atoms and cocrystallized CH2Cl2 are omitted for clarity. Selected bond lengths [Å] and angles [°] are as follows: C(1)–N(1) 1.277(11), C(1)–N(2) 1.393(11), C(2)–N(2) 1.396(11), C(2)–N(3) 1.305(11), Ni(1)–N(1) 1.947(8), Ni(1)–N(3) 1.943(8), N(1)–C(1)–N(2) 122.8(8), C(1)–N(2)–C(2) 126.2(7), N(2)–C(2)–N(3) 121.2(8), C(2)–N(3)–Ni(1) 127.5(6), N(1)–Ni(1)–N(3) 89.3(3), C(1)–N(1)–Ni(1), 127.7(6), N(1)–Ni(1)–Br(1) 102.2(3), N(1)–Ni(1)–Br(2) 120.9(3).