Table 1. Sequence Information and Analytical Data of the TEMPO-Modified RNA Sequences 3, 5, and 6.
molecular weight |
|||||
---|---|---|---|---|---|
IDa | 13C-labelsb | lengthc | yield,d nmol | calcd | found |
3 | 4 (A, C, U) | 15 | 527 | 5053.2 | 5052.2 |
5 | 1 (C) | 32 | 502 | 10361.2 | 10361.7 |
6 | 8 (C) | 27 | 480 | 8820.4 | 8820.2 |
Sequence identifier.
Number of 13C-labels (nucleotide type C = 6-13C-cytidine, U = 6-13C-uridine, A = 8-13C-adenosine).
Number of nucleotides.
Yield from 2 μmol synthesis scale.