. Author manuscript; available in PMC: 2014 Oct 23.

Published in final edited form as: J Am Chem Soc. 2013 Oct 15;135(42):10.1021/ja4092819. doi: 10.1021/ja4092819

Table 5. Scope of Amine Electrophiles with 4-Phenyl-1-butene^a.

graphic file with name nihms-532054-t0009.jpg

Isolated yields (average of two runs). 2 (1 mmol), hydroxyla-mine (1.2 mmol), Cu(OAc)₂ (2 mol %), (±)-DTBM-SEGPHOS (2.2 mol %), DEMS (2 mmol), THF (0.5 M), 40 °C, up to 36 h.

Cu(OAc)₂ (4 mol %), (±)-DTBM-SEGPHOS (4.4 mol %) were used.

Table 5. Scope of Amine Electrophiles with 4-Phenyl-1-butenea.

Table 5. Scope of Amine Electrophiles with 4-Phenyl-1-butene^a.