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. Author manuscript; available in PMC: 2014 Jul 25.
Published in final edited form as: J Med Chem. 2013 Jul 2;56(14):10.1021/jm4007615. doi: 10.1021/jm4007615

Table 1.

Selected Structural Parameters of complexes 8 and 11 obtained from X-ray single crystal diffraction studies. Bond lengths in Å and angles in °.

8 11
P(1)-N(1) 1.608(4) P(1)-N(1) 1.610(3)
N(1)-C(1) 1.469(7) N(1)-C(1) 1.463(5)
Pd(1)-N(1) 2.041(4) Pd(1)-N(1) 2.038(3)
Pd(1)-N(2) 2.025(5) Pd(1)-N(2) 2.029(3)
Pd(1)-Cl(1) 2.2938(15) Pd(1)-Cl(1) 2.3081(11)
Pd(1)-Cl(2) 2.2845(16) Pd(1)-Cl(2) 2.2895(11)
N(2)-Pd(1)-N(1) 79.51(17) N(2)-Pd(1)-N(1) 80.87(12)
Cl(2)-Pd(1)-Cl(1) 90.08(7) Cl(2)-Pd(1)-Cl(1) 90.13(4)
N(1)-Pd(1)-Cl(1) 172.28(13) N(1)-Pd(1)-Cl(1) 173.45(9)
N(2)-Pd(1)-Cl(2) 174.06(14) N(2)-Pd(1)-Cl(2) 175.94(9)
N(1)-Pd(1)-Cl(2) 97.63(13) N(1)-Pd(1)-Cl(2) 95.61(9)
N(2)-Pd(1)-Cl(1) 92.84(13) N(2)-Pd(1)-Cl(1) 93.50(9)
Fe(1)-C 2.035(6) – 2.051(7)