| Bruker SMART 1000 CCD diffractometer | 5465 independent reflections |
| Radiation source: fine-focus sealed tube | 3137 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.064 |
| φ and ω scans | θmax = 25.0°, θmin = 1.5° |
| Absorption correction: multi-scan (SADABS; Bruker, 2001) | h = −12→12 |
| Tmin = 0.784, Tmax = 0.813 | k = −14→12 |
| 8374 measured reflections | l = −14→17 |
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