| Refinement on F2 | Secondary atom site location: difference Fourier map |
| Least-squares matrix: full | Hydrogen site location: difference Fourier map |
| R[F2 > 2σ(F2)] = 0.020 | H-atom parameters constrained |
| wR(F2) = 0.051 | w = 1/[σ2(Fo2) + (0.0319P)2 + 0.5639P] where P = (Fo2 + 2Fc2)/3 |
| S = 1.06 | (Δ/σ)max = 0.001 |
| 3103 reflections | Δρmax = 1.05 e Å−3 |
| 175 parameters | Δρmin = −0.30 e Å−3 |
| 0 restraints | Absolute structure: Flack (1983), 1274 Friedel pairs |
| Primary atom site location: structure-invariant direct methods | Absolute structure parameter: −0.015 (17) |