Nonius KappaCCD with Bruker APEXII CCD area detector diffractometer | 2652 independent reflections |
Radiation source: fine-focus sealed tube | 1860 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.000 |
φ and ω scans | θmax = 26.0°, θmin = 1.6° |
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = 0→22 |
Tmin = 0.930, Tmax = 0.948 | k = 0→7 |
2652 measured reflections | l = −31→0 |