Bruker X8 Proteum diffractometer | 3296 independent reflections |
Radiation source: fine-focus rotating anode | 3267 reflections with I > 2σ(I) |
Detector resolution: 5.6 pixels mm-1 | Rint = 0.033 |
φ and ω scans | θmax = 68.2°, θmin = 5.7° |
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −10→10 |
Tmin = 0.843, Tmax = 0.956 | k = −11→14 |
25400 measured reflections | l = −21→15 |