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. 2013 Aug 23;69(Pt 9):i60. doi: 10.1107/S1600536813023106
Bruker X8 APEX diffractometer 811 independent reflections
Radiation source: fine-focus sealed tube 732 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.032
φ and ω scans θmax = 30.5°, θmin = 3.4°
Absorption correction: multi-scan (SADABS; Bruker, 2009) h = −14→13
Tmin = 0.164, Tmax = 0.376 k = −19→20
3968 measured reflections l = −9→7