Bruker SMART APEXII CCD diffractometer | 3161 independent reflections |
Radiation source: fine-focus sealed tube | 2633 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.026 |
ω and φ scans | θmax = 26.4°, θmin = 1.9° |
Absorption correction: multi-scan (SADABS; Bruker, 2008) | h = −10→10 |
Tmin = 0.966, Tmax = 0.977 | k = −10→10 |
10840 measured reflections | l = −11→13 |