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. 2013 Dec 31;2013:930787. doi: 10.1155/2013/930787

Table 1.

Comparison between CAN catalysed silent and sonic reactions.

Entry Reactions Silent conditiona Sonic conditionb
Time Yieldc Time Yieldc
1 Dimedone (1 mmol) and 2-chloro-4-fluoroaniline (1 mmol) to form 5 45 min 75% 20 min 95%
2 Reaction between intermediates 5 and 6 to give product 4 4 h 50% 1 h 90%
3 Mixing all the reactants (1, 2, and 3) 5 h 50% 1 h 90%

aIn acetonitrile (3–5 mL) at 70°C. bIn a sonic bath at 26°C (35 kHz). cIsolated yields.