TABLE 1.
| ||||
---|---|---|---|---|
entry | λmax (nm) |
Time (min.) |
Isolated yield of product (%) | |
3 | 4 | |||
1 | 254 | 45 | 33 | 10 |
2 | 300 | 90 | 63 | 13 |
3 | 350 | 135 | 30 | 5 |
4 | 300a | 45 | 56 | <1 |
Reaction was carried out in the presence of 1.0 equiv of benzophenone
| ||||
---|---|---|---|---|
entry | λmax (nm) |
Time (min.) |
Isolated yield of product (%) | |
3 | 4 | |||
1 | 254 | 45 | 33 | 10 |
2 | 300 | 90 | 63 | 13 |
3 | 350 | 135 | 30 | 5 |
4 | 300a | 45 | 56 | <1 |
Reaction was carried out in the presence of 1.0 equiv of benzophenone