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Preparation of lipid-1-P and the conjugation with GalNAc-1-P forming GalNAc-PP-lipid.
| |||
|---|---|---|---|
| Lipid | Geometry | Structure R: GalNAc | GalNAc-PP-lipids (overall yield)* |
| undecaprenol | 7 Z, 3 E |
 31 |
59% |
| heptaprenol | 4 Z, 2 E |
 32 |
36% |
| pentaprenol | 2 Z, 2 E |
 33 |
49% |
| (all-Z)-pentaprenol | 4 Z, 0 E |
 34 |
20% |
| solanesol | 0 Z, 8 E |
 35 |
50% |
| MS-pentaprenol | 1 Z, 2 E |
 36 |
26% |
overall yield is based on the polyprenols.
