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Phase diagram elucidated for the RAFT aqueous dispersion polymerization of HPMA at 50 °C using a PEG113-DB macro-CTA based on combined TEM and DLS studies. Phase regions consist of spheres (S), worms (W), unilamellar vesicles (ULV), oligolamellar vesicles (OLV), ill-defined lamellae (L), jellyfish (J), mixed phases (M), and a precipitate phase (P).
